Oxidation-affected zone in the sintered ZrB2–SiC–HfB2 composites

نویسندگان

چکیده

Understanding the behavior of ultra-high temperature ceramics (UHTCs) against oxidation is particular importance in high-temperature applications. In this study, ZrB2–SiC–HfB2 UHTC composites were fabricated by spark plasma sintering (SPS) method at different temperatures, times, and pressures to investigate effects process variables on their resistance. Before tests, as-sintered samples contained ZrB2 SiC phases with (Zr,Hf)B2 solid solution. The subjected oxidative conditions 1400 °C relative mass changes measured as a function time up 20 hours. FESEM EDS equipment used for microstructural elemental analyzes cross-sections oxide layers. Due oxygen diffusion, ZrO2 SiO2 appeared alongside (Zr, Hf)O2 surface After identifying several oxides SiC-depleted layers oxidation-affected zone, schematic model arrangement such was proposed.

برای دانلود باید عضویت طلایی داشته باشید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Weldability and Heat Affected Zone (haz) of High Energy Rate of Joining Thermoplastic Composites Using Microwaves

Industrial microwave technology for processing polymers and polymer based composites is currently in a state of considerable flux. This paper extends the applications horizon of microwaves in the area of reinforced thermoplastic composites joining, and places emphasis on the development of equipment and facilities aiming at maximising bond quality. It discusses the microwave facility used, incl...

متن کامل

Microstructure and mechanical properties of pressureless sintered alumina-silver composites

The silver toughened alumina ceramics, which were fabricated via a conventional ceramic processing route using commercially available alumina and silver oxide powders as the starting materials, exhibit a higher fracture toughness (6 to 9 MPamo.5) than the monolithic alumina ceramic ( 2.5 to 3.0 MPamo.5). The weak interfacial bonding between the silver inclusions and the alumina matrix is charac...

متن کامل

Spark Plasma Sintered Hydroxyapatite – Zirconia Composites: Structural and Mechanical Properties

Hydroxyapatite (Ca10(PO4)6(OH)2) (HAp) is a very attractive material for human tissue implantation, beacuse it makes up ~69% of the weight of bone [1]. Unfortunately HAp posses low mechanical properties (strength, fracture toughness), which is a barrier to its applications in load-bearing situations [2]. The mechanical properties of HAp composites, is based on the synthesis of composites and th...

متن کامل

Sintered Steel Composites Reinforced with Ceramic Nanoparticles: Fabrication, Characteristics and Wear Behavior

Steel composites reinforced with alumina nanoparticles were prepared by powder metallurgy process. Samples containing two different amounts of carbon (0.35 and 0.55 wt.%) and 0-5 wt.% Al2O3 nanoparticles were fabricated by mixing, compacting and sintering of diffusion bonded Distaloy AE powder. The density, hardness and wear tests were performed on the prepared samples. Fu...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

ژورنال

عنوان ژورنال: Synthesis and sintering

سال: 2022

ISSN: ['2564-0186', '2564-0194']

DOI: https://doi.org/10.53063/synsint.2022.21111